TA Instruments

AR1702-0001f

04/09/2012 15:53:52

Sample name	ASW 10 mm from base, 60 mm to top, disk 1 PMMA+Br clean
Sample notes	 
Experiment notes	Plastic parallel plate with adaptor supplied by Southampton Uni., on ETC rod with grub screws.

Distances fromlower surface of PP plate. Southampton container.
Operator	M Rides
Sample density	1.000 g/cm^3
Results file name	AR1702
Run number	1 
Results directory	D:\ARG2 rheometer\Test files\Southampton University P Stoodley May2012
Experiment was run on	04/09/2012 15:53:52

Procedure name	Flow procedure
Procedure notes	

Step name	Conditioning Step 1
Step notes	
Perform step	Yes
Initial temperature	22.4 C
Wait for correct temperature	Yes
Do set temperature	Yes
Wait for normal force	No
Perform pre-shear	No
Perform equilibration	Yes
Equilibration duration	0:01:00 hh:mm:ss
Wait for zero velocity	No
Control normal force	Uses current instrument settings
Purge gas only	No

Step name	Continuous ramp step 1
Step notes	
Perform step	Yes
Ramp type	Continuous ramp
Start controlled variable	velocity 3.000 rad/s
End controlled variable	velocity 300.0 rad/s
Duration	0:01:00 hh:mm:ss
Ramp mode	linear 
Delay time	0:00:01 hh:mm:ss
Temperature	22.4 C
Wait for temperature	No
Match duration and start value to previous step	No
Motor mode	auto 

Step name	Peak hold step
Step notes	
Perform step	Yes
Ramp type	Peak hold
Controlled variable	velocity 300.0 rad/s
Duration	0:00:30 hh:mm:ss
Delay time	0:00:01 hh:mm:ss
Temperature	22.4 C
Wait for temperature	No
Motor mode	auto 

Step name	Continuous ramp step 2
Step notes	
Perform step	Yes
Ramp type	Continuous ramp
Start controlled variable	velocity 300.0 rad/s
End controlled variable	velocity 3.000 rad/s
Duration	0:01:00 hh:mm:ss
Ramp mode	linear 
Delay time	0:00:01 hh:mm:ss
Temperature	22.4 C
Wait for temperature	No
Match duration and start value to previous step	No
Motor mode	auto 

Step name	Post-Experiment Step
Step notes	
Perform step	Yes
Do set temperature	Yes
Temperature	22.4 C
Set temperature system idle	No

Geometry name	25mm ETC plastic plate Southampton
Geometry notes	25 mm diameter parallel plastic plate with ETC rod
Geometry material	Other
Parallel plate diameter	25.00 mm
gap	10000 micro m
Gap offset	0 micro m
Geometry inertia	3.100 micro N.m.s^2
Geometry compliance	2.020E-3 rad/N.m
Gap temperature compensation	0 micro m/C
Gap temperature compensation enabled	No
Shear rate factor	1.250 
Shear stress factor	3.259E5 1/m^3
Measurement system factor	2.608E5 1/m^3
Fluid density factor	1.278E-10 m^5
Normal force factor	4074 1/m^2
Backoff distance	5000 micro m
Approximate sample volume	4.91 ml

Sample compression	linear 
Compression distance	1000.0 micro m
Compression velocity	50.0 micro m/s
Fine velocity	500.0 micro m/s
Coarse velocity	6000.0 micro m/s
Other velocity	6000.0 micro m/s
Current temperature system	Peltier plate
Temperature control	Enabled 
Purge gas only	No
Temperature calibration	Peltier plate - 0 micro m/C
	Water bath - 0 micro m/C
	Torsion oven - plate - 0 micro m/C
	Torsion oven - solid sample - 0 micro m/C
	Peltier concentric cylinders - 0 micro m/C
	None - 0 micro m/C
	Stress relaxation - 0 micro m/C
	Current temperature system - 0 micro m/C
Cooling water temperature	15.0 C
Cooling water range	6.0 C
Bearing friction correction	Yes
Bearing friction	0.262 micro N.m/(rad/s)
Bearing offset	0 micro N.m
Temperature system span and offset	Peltier plate - span 1.0000 , offset 0 C
	Water bath - span 1.0000 , offset 0 C
	Torsion oven - plate - span 1.0000 , offset 0 C
	Torsion oven - solid sample - span 1.0000 , offset 0 C
	Peltier concentric cylinders - span 1.0000 , offset 0 C
	None - span 1.0000 , offset 0 C
	Stress relaxation - span 1.0000 , offset 0 C
	Current temperature system - span 1.0000 , offset 0 C
Bearing mapping type	precision 
Number of mapping iterations	3
Instrument type (MType)	AR-G2
Firmware version	  8.29  27/10/09
Configuration version (CnfVer)	301
Parameter version (PrmVer)	301
PCB Number	*NOT_SET*
IP address	192.168.1.2
Software version	V5.8.0
Windows version	Windows XP 5.1 (Service Pack 2)
Instrument inertia	18.42 micro N.m.s^2
Auto increment run number	Yes
Prompt for file name at start of run	Yes
Auto save results file	Yes
Results file storage	Consecutive steps of same type to 1 file 
Temperature tolerance	0.2 C
Temperature duration	0:00:10 hh:mm:ss
Wait for temperature even if OK	Yes
Gap tolerance	4 micro m
Gap duration	0:00:02 hh:mm:ss
Override wait for gap	No
Velocity tolerance	0.1000 rad/s
Zero speed after pre-shear	Leave as is 
Zero normal force before run	No
Zero timer before run	Before pre-shear 
Non-equilibrium minimum velocity	1.000E-4 rad/s
Zero strain at the start of each flow step	Yes
Inertia correction	Yes
Collect negative shear rate data if stress is positive	Yes
Collect all points	No
Display flow point graph during run	Yes
Store flow point graph with results	Yes
Store images to the results for flow steps	Yes
Creep zero displacement	Yes
Store images to the results for creep steps	Yes
Standard creep image store frequency	10 s
Repeated creep image store frequency in repeats	10 
Display oscillation waveform graph during run	Yes
Store oscillation waveform graph with results	Yes
Display strain control tries during run	Yes
Store strain control tries with results	Yes
Store images to the results for oscillation steps	Yes
Stress relaxation zero displacement	Yes
Store images to the results for stress relaxation steps	Yes
Flow torque limit	10.00 micro N.m
Flow velocity limit	1.000E-3 rad/s
Oscillation torque limit	5.00 micro N.m
Oscillation displacement limit	1.00E-5 rad
Oscillation raw phase limit	170.0 degrees
Oscillation minimum normal force limit	0.1000 N
Oscillation maximum normal force limit	50.00 N
Flow velocity tolerance	1.00 %
Oscillation torque tolerance	1.00 %
Oscillation displacement tolerance	1.00 %
Oscillation velocity tolerance	1.00 %
Temperature tolerance	1.0 C

Continuous ramp step 1

shear stress	shear rate	viscosity	time	temperature	normal stress	displacement	gap	normal force	normal stress coefficient	strain	% strain	1/temperature	time	time global	time global	torque	velocity
Pa	1/s	Pa.s	s	C	Pa	rad	micro m	N	Pa.s^2			1/K	min	min	s	micro N.m	rad/s

-22.88	7.388	-3.097	1.0120	22.4	767.1	5.3199	10000	0.1883	14.05	6.6499	664.99	3.384E-3	0.0	1.0	61.012	-70.202	5.910
1.217	12.24	0.09944	2.0160	22.4	772.1	13.4919	10000	0.1895	5.153	16.865	1686.5	3.384E-3	0.0	1.0	62.016	3.7342	9.793
1.504	19.30	0.07792	3.0120	22.4	773.7	26.7477	10000	0.1899	2.078	33.435	3343.5	3.384E-3	0.1	1.1	63.012	4.6131	15.44
2.025	22.99	0.08808	4.0120	22.4	746.5	40.7234	10000	0.1832	1.413	50.904	5090.4	3.384E-3	0.1	1.1	64.012	6.2115	18.39
3.261	30.81	0.1058	5.0160	22.4	766.3	67.4427	10000	0.1881	0.8070	84.303	8430.3	3.383E-3	0.1	1.1	65.016	10.006	24.65
5.113	39.46	0.1296	6.0160	22.4	772.1	106.6970	10000	0.1895	0.4958	133.37	13337	3.384E-3	0.1	1.1	66.016	15.685	31.57
5.824	42.51	0.1370	7.0120	22.4	753.1	126.1920	10000	0.1848	0.4166	157.74	15774	3.383E-3	0.1	1.1	67.012	17.866	34.01
7.224	49.11	0.1471	8.0120	22.4	762.2	165.1360	10000	0.1871	0.3160	206.42	20642	3.384E-3	0.1	1.1	68.012	22.163	39.29
9.402	57.53	0.1634	8.9960	22.4	762.2	223.0650	10000	0.1871	0.2303	278.83	27883	3.383E-3	0.1	1.1	68.996	28.846	46.02
11.60	63.68	0.1821	9.9960	22.4	761.3	274.6530	10000	0.1869	0.1877	343.32	34332	3.384E-3	0.2	1.2	69.996	35.583	50.95
13.36	69.65	0.1918	10.996	22.4	770.4	325.9710	10000	0.1891	0.1588	407.46	40746	3.384E-3	0.2	1.2	70.996	40.982	55.72
15.06	75.12	0.2005	12.012	22.4	750.6	377.1600	10000	0.1842	0.1330	471.45	47145	3.383E-3	0.2	1.2	72.012	46.216	60.09
17.10	80.51	0.2124	13.012	22.4	744.0	434.6990	10000	0.1826	0.1148	543.37	54337	3.383E-3	0.2	1.2	73.012	52.463	64.41
19.42	86.43	0.2246	14.012	22.4	739.0	498.5670	10000	0.1814	0.09893	623.21	62321	3.384E-3	0.2	1.2	74.012	59.567	69.14
22.13	94.60	0.2340	14.996	22.4	731.6	594.1480	10000	0.1796	0.08175	742.69	74269	3.383E-3	0.2	1.2	74.996	67.907	75.68
24.21	99.91	0.2424	16.012	22.4	734.9	664.2390	10000	0.1804	0.07362	830.30	83030	3.383E-3	0.3	1.3	76.012	74.288	79.93
26.65	105.7	0.2522	17.008	22.4	737.4	740.6220	10000	0.1810	0.06605	925.78	92578	3.383E-3	0.3	1.3	77.008	81.770	84.53
30.20	113.7	0.2655	18.000	22.4	729.1	855.0430	10000	0.1789	0.05637	1068.8	1.0688E5	3.383E-3	0.3	1.3	78.000	92.638	90.98
32.14	118.8	0.2706	19.008	22.4	725.8	931.2050	10000	0.1781	0.05143	1164.0	1.1640E5	3.383E-3	0.3	1.3	79.008	98.616	95.04
34.36	124.3	0.2765	20.016	22.4	725.8	1020.1300	10000	0.1781	0.04701	1275.2	1.2752E5	3.383E-3	0.3	1.3	80.016	105.41	99.40
38.05	132.3	0.2877	21.000	22.4	721.7	1154.0300	10000	0.1771	0.04124	1442.5	1.4425E5	3.384E-3	0.4	1.4	81.000	116.75	105.8
40.56	137.4	0.2952	22.000	22.4	736.5	1242.1000	10000	0.1808	0.03903	1552.6	1.5526E5	3.384E-3	0.4	1.4	82.000	124.43	109.9
43.38	142.8	0.3038	22.996	22.4	720.0	1344.1600	10000	0.1767	0.03531	1680.2	1.6802E5	3.384E-3	0.4	1.4	82.996	133.10	114.2
46.87	150.8	0.3108	24.016	22.4	724.1	1496.2800	10000	0.1777	0.03184	1870.4	1.8704E5	3.384E-3	0.4	1.4	84.016	143.79	120.6
49.33	155.9	0.3164	24.996	22.4	707.6	1596.8700	10000	0.1737	0.02911	1996.1	1.9961E5	3.383E-3	0.4	1.4	84.996	151.33	124.7
52.13	161.3	0.3231	26.000	22.4	711.7	1710.9200	10000	0.1747	0.02735	2138.7	2.1387E5	3.383E-3	0.4	1.4	86.000	159.92	129.1
56.20	169.3	0.3319	27.012	22.4	713.4	1881.8500	10000	0.1751	0.02488	2352.3	2.3523E5	3.384E-3	0.5	1.5	87.012	172.42	135.5
59.32	174.4	0.3400	27.996	22.4	691.1	1995.7200	10000	0.1696	0.02271	2494.7	2.4947E5	3.384E-3	0.5	1.5	87.996	181.98	139.6
62.92	179.6	0.3504	29.004	22.4	693.6	2116.0100	10000	0.1702	0.02151	2645.0	2.6450E5	3.384E-3	0.5	1.5	89.004	193.04	143.6
66.99	187.5	0.3572	30.024	22.4	701.0	2305.6799	10000	0.1721	0.01993	2882.1	2.8821E5	3.384E-3	0.5	1.5	90.024	205.51	150.0
69.98	192.7	0.3632	31.012	22.4	691.1	2432.9900	10000	0.1696	0.01861	3041.2	3.0412E5	3.384E-3	0.5	1.5	91.012	214.69	154.2
72.66	200.5	0.3623	32.012	22.4	689.4	2635.1799	10000	0.1692	0.01714	3294.0	3.2940E5	3.384E-3	0.5	1.5	92.012	222.90	160.4
78.66	205.8	0.3822	33.012	22.4	682.0	2773.7000	10000	0.1674	0.01610	3467.1	3.4671E5	3.384E-3	0.6	1.6	93.012	241.32	164.7
80.63	211.0	0.3822	34.000	22.4	665.5	2912.6499	10000	0.1633	0.01495	3640.8	3.6408E5	3.383E-3	0.6	1.6	94.000	247.37	168.8
85.00	218.6	0.3888	35.020	22.4	671.2	3127.4700	10000	0.1647	0.01405	3909.3	3.9093E5	3.383E-3	0.6	1.6	95.020	260.77	174.9
89.15	223.9	0.3982	36.012	22.4	659.7	3279.8999	10000	0.1619	0.01316	4099.9	4.0999E5	3.383E-3	0.6	1.6	96.012	273.52	179.1
92.07	229.1	0.4019	37.016	22.4	656.4	3510.6299	10000	0.1611	0.01251	4388.3	4.3883E5	3.384E-3	0.6	1.6	97.016	282.47	183.3
96.80	236.6	0.4091	38.016	22.4	655.5	3657.9900	10000	0.1609	0.01171	4572.5	4.5725E5	3.384E-3	0.6	1.6	98.016	296.97	189.3
100.3	241.8	0.4146	39.012	22.4	647.3	3822.3000	10000	0.1589	0.01107	4777.9	4.7779E5	3.384E-3	0.7	1.7	99.012	307.64	193.5
106.2	249.6	0.4255	39.996	22.4	633.2	4068.4800	10000	0.1554	0.01017	5085.6	5.0856E5	3.384E-3	0.7	1.7	99.996	325.78	199.7
109.1	254.6	0.4285	40.996	22.4	654.7	4232.6401	10000	0.1607	0.01010	5290.8	5.2908E5	3.384E-3	0.7	1.7	100.996	334.70	203.7
112.3	259.8	0.4323	42.008	22.4	627.4	4500.7300	10000	0.1540	9.293E-3	5625.9	5.6259E5	3.384E-3	0.7	1.7	102.008	344.63	207.9
118.1	267.6	0.4412	43.012	22.4	632.4	4674.5601	10000	0.1552	8.830E-3	5843.2	5.8432E5	3.383E-3	0.7	1.7	103.012	362.25	214.1
121.2	272.7	0.4446	44.012	22.4	624.1	4851.2798	10000	0.1532	8.394E-3	6064.1	6.0641E5	3.383E-3	0.7	1.7	104.012	371.95	218.1
127.0	280.3	0.4530	45.012	22.4	618.3	5128.8799	10000	0.1518	7.867E-3	6411.1	6.4111E5	3.384E-3	0.8	1.8	105.012	389.62	224.3
128.9	285.5	0.4514	46.012	22.4	626.6	5320.0400	10000	0.1538	7.686E-3	6650.1	6.6501E5	3.384E-3	0.8	1.8	106.012	395.44	228.4
135.2	293.1	0.4613	47.012	22.4	625.8	5603.1201	10000	0.1536	7.284E-3	7003.9	7.0039E5	3.384E-3	0.8	1.8	107.012	414.84	234.5
139.1	298.1	0.4667	47.996	22.4	605.9	5797.6602	10000	0.1487	6.817E-3	7247.1	7.2471E5	3.384E-3	0.8	1.8	107.996	426.85	238.5
143.8	303.3	0.4742	49.012	22.4	601.8	5999.5000	10000	0.1477	6.541E-3	7499.4	7.4994E5	3.384E-3	0.8	1.8	109.012	441.25	242.7
148.8	311.0	0.4785	50.016	22.4	619.2	6302.3301	10000	0.1520	6.403E-3	7877.9	7.8779E5	3.384E-3	0.8	1.8	110.016	456.49	248.8
153.5	316.0	0.4857	51.012	22.4	601.0	6510.5898	10000	0.1475	6.018E-3	8138.2	8.1382E5	3.384E-3	0.9	1.9	111.012	470.88	252.8
161.4	323.8	0.4986	52.012	22.4	576.2	6832.0200	10000	0.1414	5.496E-3	8540.0	8.5400E5	3.384E-3	0.9	1.9	112.012	495.28	259.0
165.0	328.9	0.5017	53.012	22.4	577.0	7046.5801	10000	0.1416	5.335E-3	8808.2	8.8082E5	3.384E-3	0.9	1.9	113.012	506.19	263.1
173.4	336.4	0.5155	53.996	22.4	567.9	7374.4902	10000	0.1394	5.018E-3	9218.1	9.2181E5	3.383E-3	0.9	1.9	113.996	532.08	269.1
174.8	341.6	0.5117	55.016	22.4	574.5	7601.5498	10000	0.1410	4.924E-3	9501.9	9.5019E5	3.383E-3	0.9	1.9	115.016	536.26	273.3
177.5	346.7	0.5120	56.012	22.4	579.5	7831.0298	10000	0.1422	4.821E-3	9788.8	9.7888E5	3.383E-3	0.9	1.9	116.012	544.55	277.4
187.2	354.2	0.5284	56.996	22.4	568.7	8168.9199	10000	0.1396	4.533E-3	10211	1.0211E6	3.383E-3	0.9	1.9	116.996	574.24	283.4
189.5	359.3	0.5273	58.012	22.4	569.6	8408.5098	10000	0.1398	4.411E-3	10511	1.0511E6	3.384E-3	1.0	2.0	118.012	581.29	287.5
195.1	367.0	0.5316	59.012	22.4	548.9	8767.7197	10000	0.1347	4.075E-3	10960	1.0960E6	3.384E-3	1.0	2.0	119.012	598.59	293.6
197.7	372.0	0.5313	59.996	22.4	563.8	9007.2100	10000	0.1384	4.074E-3	11259	1.1259E6	3.384E-3	1.0	2.0	119.996	606.41	297.6

Peak hold step

shear stress	shear rate	viscosity	time	temperature	normal stress	displacement	gap	normal force	normal stress coefficient	strain	% strain	1/temperature	time	time global	time global	torque	velocity
Pa	1/s	Pa.s	s	C	Pa	rad	micro m	N	Pa.s^2			1/K	min	min	s	micro N.m	rad/s

201.1	375.0	0.5362	1.0040	22.4	558.8	316.4340	10000	0.1372	3.974E-3	395.54	39554	3.384E-3	0.0	2.0	121.004	616.85	300.0
205.1	375.0	0.5470	2.0240	22.4	539.8	566.3360	10000	0.1325	3.839E-3	707.92	70792	3.384E-3	0.0	2.0	122.024	629.31	300.0
202.1	375.0	0.5389	3.0240	22.4	551.4	817.7630	10000	0.1353	3.921E-3	1022.2	1.0222E5	3.384E-3	0.1	2.1	123.024	619.98	300.0
204.4	375.0	0.5449	4.0040	22.4	531.5	1194.8101	10000	0.1305	3.780E-3	1493.5	1.4935E5	3.384E-3	0.1	2.1	124.004	626.96	300.0
203.7	375.0	0.5431	5.0200	22.4	510.9	1446.0800	10000	0.1254	3.633E-3	1807.6	1.8076E5	3.384E-3	0.1	2.1	125.020	624.85	300.0
207.2	375.0	0.5527	6.0080	22.4	520.8	1825.7500	10000	0.1278	3.704E-3	2282.2	2.2822E5	3.384E-3	0.1	2.1	126.008	635.83	300.0
200.9	375.0	0.5356	7.0040	22.4	579.5	2074.3501	10000	0.1422	4.120E-3	2592.9	2.5929E5	3.384E-3	0.1	2.1	127.004	616.23	300.0
202.8	375.0	0.5408	8.0040	22.4	549.7	2325.7900	10000	0.1349	3.909E-3	2907.2	2.9072E5	3.384E-3	0.1	2.1	128.004	622.20	300.0
200.0	375.0	0.5334	9.0200	22.4	572.0	2702.8000	10000	0.1404	4.068E-3	3378.5	3.3785E5	3.384E-3	0.2	2.2	129.020	613.66	300.0
203.9	375.0	0.5438	10.004	22.4	554.7	2954.0701	10000	0.1361	3.944E-3	3692.6	3.6926E5	3.384E-3	0.2	2.2	130.004	625.69	300.0
201.6	375.0	0.5376	11.028	22.4	572.9	3205.4800	10000	0.1406	4.074E-3	4006.9	4.0069E5	3.384E-3	0.2	2.2	131.028	618.54	300.0
203.5	375.0	0.5427	12.008	22.4	558.8	3583.9199	10000	0.1372	3.974E-3	4479.9	4.4799E5	3.384E-3	0.2	2.2	132.008	624.34	300.0
200.2	375.0	0.5338	13.004	22.4	583.6	3833.6299	10000	0.1432	4.150E-3	4792.0	4.7920E5	3.383E-3	0.2	2.2	133.004	614.15	300.0
203.9	375.0	0.5437	14.020	22.4	534.8	4211.8999	10000	0.1313	3.803E-3	5264.9	5.2649E5	3.384E-3	0.2	2.2	134.020	625.47	300.0
198.8	375.0	0.5302	15.020	22.4	582.8	4468.0801	10000	0.1430	4.145E-3	5585.1	5.5851E5	3.383E-3	0.3	2.3	135.020	609.98	300.0
204.5	375.0	0.5452	16.020	22.4	519.1	4713.4199	10000	0.1274	3.692E-3	5891.8	5.8918E5	3.383E-3	0.3	2.3	136.020	627.26	300.0
203.1	375.0	0.5417	17.020	22.4	524.9	5090.4302	10000	0.1288	3.733E-3	6363.0	6.3630E5	3.383E-3	0.3	2.3	137.020	623.17	300.0
202.1	375.0	0.5388	18.004	22.4	527.4	5341.6899	10000	0.1294	3.751E-3	6677.1	6.6771E5	3.383E-3	0.3	2.3	138.004	619.92	300.0
204.6	375.0	0.5457	19.008	22.4	539.0	5720.8301	10000	0.1323	3.833E-3	7151.0	7.1510E5	3.383E-3	0.3	2.3	139.008	627.85	300.0
200.1	375.0	0.5336	20.020	22.4	525.8	5969.9302	10000	0.1290	3.738E-3	7462.4	7.4624E5	3.383E-3	0.3	2.3	140.020	613.88	300.0
201.6	375.0	0.5375	21.004	22.4	551.4	6221.3599	10000	0.1353	3.921E-3	7776.7	7.7767E5	3.383E-3	0.4	2.4	141.004	618.41	300.0
201.4	375.0	0.5371	22.004	22.4	568.7	6598.3999	10000	0.1396	4.045E-3	8248.0	8.2480E5	3.384E-3	0.4	2.4	142.004	617.89	300.0
201.4	375.0	0.5372	23.008	22.4	553.0	6850.8999	10000	0.1357	3.933E-3	8563.6	8.5636E5	3.384E-3	0.4	2.4	143.008	618.03	300.0
199.5	375.0	0.5321	24.008	22.4	559.6	7101.0000	10000	0.1374	3.980E-3	8876.3	8.8763E5	3.384E-3	0.4	2.4	144.008	612.15	300.0
199.0	375.0	0.5305	25.000	22.4	583.6	7480.5898	10000	0.1432	4.150E-3	9350.7	9.3507E5	3.384E-3	0.4	2.4	145.000	610.41	300.0
201.1	375.0	0.5363	26.020	22.4	553.9	7729.1802	10000	0.1359	3.939E-3	9661.5	9.6615E5	3.383E-3	0.4	2.4	146.020	616.99	300.0
202.8	375.0	0.5409	27.004	22.4	553.9	8106.3101	10000	0.1359	3.938E-3	10133	1.0133E6	3.383E-3	0.5	2.5	147.004	622.33	300.0
204.4	375.0	0.5452	28.004	22.4	544.8	8358.8496	10000	0.1337	3.874E-3	10449	1.0449E6	3.383E-3	0.5	2.5	148.004	627.20	300.0
206.6	375.0	0.5508	29.004	22.4	520.8	8611.5000	10000	0.1278	3.703E-3	10764	1.0764E6	3.383E-3	0.5	2.5	149.004	633.72	300.0
202.0	375.0	0.5386	30.004	22.4	551.4	8987.2305	10000	0.1353	3.921E-3	11234	1.1234E6	3.383E-3	0.5	2.5	150.004	619.65	300.0

Continuous ramp step 2

shear stress	shear rate	viscosity	time	temperature	normal stress	displacement	gap	normal force	normal stress coefficient	strain	% strain	1/temperature	time	time global	time global	torque	velocity
Pa	1/s	Pa.s	s	C	Pa	rad	micro m	N	Pa.s^2			1/K	min	min	s	micro N.m	rad/s

202.2	371.9	0.5438	1.0120	22.4	540.6	230.0370	10000	0.1327	3.910E-3	287.55	28755	3.383E-3	0.0	2.5	152.012	620.38	297.5
194.3	364.4	0.5333	2.0120	22.4	568.7	585.5150	10000	0.1396	4.284E-3	731.89	73189	3.384E-3	0.0	2.6	153.012	596.13	291.5
191.0	359.3	0.5316	3.0120	22.4	553.9	833.5470	10000	0.1359	4.291E-3	1041.9	1.0419E5	3.384E-3	0.1	2.6	154.012	585.88	287.4
183.7	351.6	0.5225	4.0120	22.4	558.8	1174.2400	10000	0.1372	4.521E-3	1467.8	1.4678E5	3.384E-3	0.1	2.6	155.012	563.59	281.3
177.3	346.6	0.5114	4.9960	22.4	564.6	1399.5699	10000	0.1386	4.700E-3	1749.5	1.7495E5	3.384E-3	0.1	2.6	155.996	543.81	277.3
178.1	341.5	0.5216	6.0120	22.4	549.7	1739.8500	10000	0.1349	4.713E-3	2174.8	2.1748E5	3.384E-3	0.1	2.6	157.012	546.52	273.2
167.0	333.8	0.5005	7.0120	22.4	611.7	1963.0100	10000	0.1501	5.492E-3	2453.8	2.4538E5	3.384E-3	0.1	2.6	158.012	512.48	267.0
162.6	328.7	0.4947	8.0120	22.4	589.4	2175.9800	10000	0.1447	5.454E-3	2720.0	2.7200E5	3.384E-3	0.1	2.7	159.012	498.92	263.0
153.2	321.1	0.4769	9.0080	22.4	628.3	2495.3701	10000	0.1542	6.092E-3	3119.2	3.1192E5	3.384E-3	0.2	2.7	160.008	469.87	256.9
152.8	316.0	0.4836	9.9960	22.4	615.0	2707.9800	10000	0.1510	6.161E-3	3385.0	3.3850E5	3.383E-3	0.2	2.7	160.996	468.75	252.8
148.9	308.3	0.4830	11.016	22.4	608.4	3014.8101	10000	0.1493	6.402E-3	3768.5	3.7685E5	3.384E-3	0.2	2.7	162.016	456.84	246.6
140.7	303.2	0.4639	12.152	22.4	642.3	3216.8601	10000	0.1576	6.986E-3	4021.1	4.0211E5	3.384E-3	0.2	2.7	163.152	431.55	242.6
143.4	298.0	0.4811	13.000	22.4	605.1	3415.3501	10000	0.1485	6.812E-3	4269.2	4.2692E5	3.384E-3	0.2	2.7	164.000	439.90	238.4
135.7	290.4	0.4672	13.996	22.4	625.8	3703.1201	10000	0.1536	7.420E-3	4628.9	4.6289E5	3.384E-3	0.2	2.7	164.996	416.29	232.3
130.3	285.4	0.4565	14.996	22.4	625.8	3895.3301	10000	0.1536	7.685E-3	4869.2	4.8692E5	3.383E-3	0.2	2.8	165.996	399.66	228.3
126.3	277.6	0.4549	16.008	22.4	616.7	4172.2798	10000	0.1514	8.001E-3	5215.4	5.2154E5	3.383E-3	0.3	2.8	167.008	387.44	222.1
120.5	272.4	0.4421	17.008	22.4	637.3	4353.7700	10000	0.1564	8.587E-3	5442.2	5.4422E5	3.384E-3	0.3	2.8	168.008	369.54	218.0
117.8	267.4	0.4404	17.992	22.4	646.4	4617.2700	10000	0.1587	9.040E-3	5771.6	5.7716E5	3.384E-3	0.3	2.8	168.992	361.33	213.9
112.6	259.7	0.4335	18.992	22.4	642.3	4791.5000	10000	0.1576	9.523E-3	5989.4	5.9894E5	3.384E-3	0.3	2.8	169.992	345.38	207.8
109.4	254.4	0.4298	20.008	22.4	653.1	4966.6499	10000	0.1603	0.01009	6208.3	6.2083E5	3.384E-3	0.3	2.9	171.008	335.54	203.6
103.9	246.8	0.4210	21.012	22.4	658.8	5210.5200	10000	0.1617	0.01082	6513.2	6.5132E5	3.384E-3	0.4	2.9	172.012	318.77	197.4
102.2	241.7	0.4228	22.008	22.4	653.1	5373.1099	10000	0.1603	0.01118	6716.4	6.7164E5	3.383E-3	0.4	2.9	173.008	313.48	193.3
96.89	236.4	0.4098	22.996	22.4	642.3	5538.7500	10000	0.1576	0.01149	6923.4	6.9234E5	3.383E-3	0.4	2.9	173.996	297.24	189.1
92.29	228.8	0.4034	24.012	22.4	667.1	5760.7300	10000	0.1637	0.01274	7200.9	7.2009E5	3.384E-3	0.4	2.9	175.012	283.15	183.1
88.06	223.7	0.3936	25.040	22.4	677.0	5910.6401	10000	0.1662	0.01353	7388.3	7.3883E5	3.384E-3	0.4	2.9	176.040	270.15	179.0
83.39	215.8	0.3864	25.996	22.4	677.0	6135.6001	10000	0.1662	0.01454	7669.5	7.6695E5	3.384E-3	0.4	2.9	176.996	255.82	172.6
80.43	210.7	0.3818	26.988	22.4	669.6	6272.9399	10000	0.1643	0.01509	7841.2	7.8412E5	3.384E-3	0.4	3.0	177.988	246.76	168.5
77.65	205.6	0.3777	28.000	22.4	680.3	6480.6802	10000	0.1670	0.01610	8100.9	8.1009E5	3.384E-3	0.5	3.0	179.000	238.21	164.5
72.70	197.7	0.3678	28.992	22.4	679.5	6616.5200	10000	0.1668	0.01739	8270.7	8.2707E5	3.384E-3	0.5	3.0	179.992	223.06	158.1
68.68	192.6	0.3566	29.996	22.4	691.1	6741.2900	10000	0.1696	0.01863	8426.6	8.4266E5	3.383E-3	0.5	3.0	180.996	210.70	154.1
63.98	184.9	0.3460	31.008	22.4	696.9	6928.7300	10000	0.1710	0.02038	8660.9	8.6609E5	3.384E-3	0.5	3.0	182.008	196.29	147.9
62.04	179.6	0.3454	32.012	22.4	687.8	7053.4399	10000	0.1688	0.02132	8816.8	8.8168E5	3.384E-3	0.5	3.1	183.012	190.34	143.7
58.49	174.3	0.3356	33.008	22.4	709.3	7171.9800	10000	0.1741	0.02335	8965.0	8.9650E5	3.384E-3	0.6	3.1	184.008	179.45	139.4
55.28	166.6	0.3317	33.996	22.4	710.1	7341.7300	10000	0.1743	0.02557	9177.2	9.1772E5	3.384E-3	0.6	3.1	184.996	169.61	133.3
52.70	161.4	0.3266	34.996	22.4	720.0	7452.7798	10000	0.1767	0.02766	9316.0	9.3160E5	3.383E-3	0.6	3.1	185.996	161.69	129.1
48.96	155.9	0.3141	36.012	22.4	730.8	7564.9199	10000	0.1794	0.03008	9456.2	9.4562E5	3.383E-3	0.6	3.1	187.012	150.20	124.7
45.13	148.1	0.3048	36.996	22.4	723.3	7714.5601	10000	0.1775	0.03298	9643.2	9.6432E5	3.383E-3	0.6	3.1	187.996	138.47	118.5
42.60	142.8	0.2984	38.012	22.4	724.1	7814.2900	10000	0.1777	0.03551	9767.9	9.7679E5	3.383E-3	0.6	3.2	189.012	130.71	114.2
39.63	137.3	0.2886	39.008	22.4	721.7	7914.6699	10000	0.1771	0.03828	9893.3	9.8933E5	3.383E-3	0.7	3.2	190.008	121.57	109.8
35.94	129.5	0.2774	40.008	22.4	723.3	8044.5298	10000	0.1775	0.04311	10056	1.0056E6	3.383E-3	0.7	3.2	191.008	110.25	103.6
33.63	124.2	0.2707	40.996	22.4	734.1	8131.7202	10000	0.1802	0.04757	10165	1.0165E6	3.383E-3	0.7	3.2	191.996	103.17	99.38
31.82	118.7	0.2681	42.012	22.4	728.3	8218.6104	10000	0.1787	0.05171	10273	1.0273E6	3.384E-3	0.7	3.2	193.012	97.610	94.94
27.87	110.9	0.2513	43.008	22.4	734.9	8330.5596	10000	0.1804	0.05972	10413	1.0413E6	3.384E-3	0.7	3.2	194.008	85.508	88.74
26.43	105.6	0.2503	43.988	22.4	728.3	8405.0801	10000	0.1787	0.06531	10506	1.0506E6	3.384E-3	0.7	3.2	194.988	81.080	84.48
23.51	99.99	0.2351	45.008	22.4	739.9	8479.4697	10000	0.1816	0.07399	10599	1.0599E6	3.384E-3	0.8	3.3	196.008	72.127	80.00
20.42	91.74	0.2226	45.992	22.4	738.2	8579.7695	10000	0.1812	0.08771	10725	1.0725E6	3.383E-3	0.8	3.3	196.992	62.653	73.39
18.41	86.35	0.2132	47.008	22.4	722.5	8640.6602	10000	0.1773	0.09689	10801	1.0801E6	3.384E-3	0.8	3.3	198.008	56.469	69.08
16.24	80.62	0.2014	47.992	22.4	759.7	8702.4004	10000	0.1865	0.1169	10878	1.0878E6	3.383E-3	0.8	3.3	198.992	49.814	64.50
14.57	74.78	0.1948	48.996	22.4	752.3	8757.9102	10000	0.1846	0.1345	10947	1.0947E6	3.384E-3	0.8	3.3	199.996	44.694	59.83
12.78	69.48	0.1839	49.992	22.4	748.1	8807.2695	10000	0.1836	0.1549	11009	1.1009E6	3.384E-3	0.8	3.3	200.992	39.207	55.59
11.15	63.76	0.1749	51.008	22.4	751.4	8856.4902	10000	0.1844	0.1848	11071	1.1071E6	3.384E-3	0.9	3.4	202.008	34.208	51.01
9.281	57.49	0.1614	51.992	22.4	754.7	8924.2598	10000	0.1852	0.2283	11155	1.1155E6	3.384E-3	0.9	3.4	202.992	28.475	46.00
7.290	49.04	0.1487	53.008	22.4	742.3	8960.6299	10000	0.1822	0.3087	11201	1.1201E6	3.383E-3	0.9	3.4	204.008	22.366	39.23
5.748	42.88	0.1340	54.012	22.4	762.2	8997.1904	10000	0.1871	0.4145	11246	1.1246E6	3.383E-3	0.9	3.4	205.012	17.636	34.31
4.546	36.40	0.1249	55.008	22.4	757.2	9027.3203	10000	0.1858	0.5714	11284	1.1284E6	3.384E-3	0.9	3.4	206.008	13.948	29.12
3.466	30.82	0.1125	55.992	22.4	766.3	9051.8896	10000	0.1881	0.8067	11315	1.1315E6	3.384E-3	0.9	3.4	206.992	10.634	24.66
2.893	27.64	0.1047	56.992	22.4	768.8	9063.3799	10000	0.1887	1.006	11329	1.1329E6	3.384E-3	0.9	3.5	207.992	8.8766	22.11
1.730	20.01	0.08648	57.992	22.4	774.6	9086.3896	10000	0.1901	1.935	11358	1.1358E6	3.384E-3	1.0	3.5	208.992	5.3083	16.01
0.8818	13.44	0.06561	58.992	22.4	766.3	9097.8604	10000	0.1881	4.242	11372	1.1372E6	3.383E-3	1.0	3.5	209.992	2.7052	10.75
0.2362	6.066	0.03895	59.992	22.4	759.7	9105.5195	10000	0.1865	20.65	11382	1.1382E6	3.383E-3	1.0	3.5	210.992	0.72477	4.852

